应用间隔流动分析仪测定土壤硝态氮和亚硝态氮含量
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国家科技支撑计划重大项目(2012BAD04B02-2)


Soil nitrate and nitrite content determined by Skalar SAN++
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    摘要:

    使用SAN++间隔流动分析仪,研究了测定土壤硝酸盐和亚硝酸盐的新方法。结果表明,SAN++间隔流动分析仪在测定土壤中NO-3-N和NO-2-N含量时标准曲线相关系数均在0.999 5以上,检测限分别为N 0.20 mg/kg和20.00 μg/kg,回收率在98.0%~101.8%之间,相对标准偏差在0.95%~2.25%之间,具有较高的精密度、准确度。该方法使用2.0 mol/L KCl溶液作为浸提剂,适用于吉林省不同土壤类型,并具有线性范围宽、分析速度快、样品用量少、自动化程度高和同时测定土壤中NO-3-N和NO-2-N等优点。

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    This study reported a new method of the Skalar SAN++ to determine soil nitrate and nitrite contents.The result showed that the correlation coefficient of the standard curve was greater than 0.999 5 when the soil NO-3-N and NO-2-N contents were determined with the Skalar SAN++.The detection limits were N 0.20 mg/kg and N 20.00 μg/kg.The added recovery rate was between 98.0%~101.8%,the relative standard deviation(RSD)was between 0.95%~2.25%,and the method had high precision and accuracy.This method used 2.0 mol/L KCl as solution agent was suitable for different soils of Jilin province.The method had a wide linear range,fast,low sample consumption,high degree of automation and determined both soil NO-3- N and NO-2-N content simultaneously.

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杨靖民,张忠庆,曹国军.应用间隔流动分析仪测定土壤硝态氮和亚硝态氮含量[J].中国土壤与肥料,2014,(2):101-105.

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  • 收稿日期:2013-05-17
  • 最后修改日期:2013-06-07
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  • 在线发布日期: 2014-04-14
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